Nickel (EHC 108, 1991) - INCHEM
Synthesis of compound 1-4: Organotin(IV) compounds with dithiocarbamate ligand are extensively being synthesized due to their potential in various fields including chemotherapeutic drugs. Organotin(IV) compounds derived from butylphenyldithiocarbamate series have not yet been synthesized, characterized and currently reported by any researchers. In this study, four types of organotin(IV) butylphenyldithiocarbamate compounds were successfully synthesized using direct method in 1:2 and 1:1 mole ratios for diorganotin (IV) and triorganotin (IV) compounds, respectively. All compounds were in agreement with the suggested molecular formula:
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Synthesis of compound 1-4: All compounds were successfully synthesized using method. The general reaction scheme of diorganotin (IV) butylphenyldithiocarbamate preparation was given in . The physical and analytical data for compound 1-4 were given in .
The IUPAC Subcommittee on the Environmental and Occupational Toxicology of Nickel (Sunderman, 1980) developed a reference method for the determination of nickel in serum or urine by EAAS, after acid digestion and the subsequent extraction of nickel with ammonium pyrrolidine dithiocarbamate (APDC) into methyl isobutyl ketone (MIBK).
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and and (2011)Synthesis, characterization and cytotoxic activity of palladium (II) dithiocarbamate complexes with α,ω-diamines. Inorganica Chimica Acta, 376 (1). pp. 574-580. ISSN 0020-1693