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Edited By: Dionissios Mantzavinos

Nitrogen-doped carbon nanotubes are selective and robust electrocatalysts for CO2 reduction to formate in aqueous media without the use of a metal catalyst. Polyethylenimine (PEI) functions as a co-catalyst by significantly reducing catalytic overpotential and increasing current density and efficiency. The co-catalysis appears to help in stabilizing the singly reduced intermediate CO2•– and concentrating CO2 in the PEI overlayer.

Edited By: Dionissios Mantzavinos

Materials preparation, electrochemical measurements, and physical characterizations. This material is available free of charge via the Internet at .

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